HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridinium chloride → 3-(3,5-Dimethyl-4-hydroxybenzoyl)-2-phenylbenzofuran
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridinium chloride | HCID 10176127 | — |
| Reactant | 3-(3,5-Dimethyl-4-methoxybenzoyl)-2-phenylbenzofuran | HCID 21435358 | — |
| Product | 3-(3,5-Dimethyl-4-hydroxybenzoyl)-2-phenylbenzofuran | HCID 21435273 | — |
Reaction Steps
3-(3,5-Dimethyl-4-methoxybenzoyl)-2-phenylbenzofuran (17.8 g., 0.05 mol.) is combined with 50 g. of freshly distilled pyridine hydrochloride and the mixture is refluxed 1 hour. The hot mixture is poured with stirring onto an ice-dilute hydrochloric acid mixture and the precipitate is collected to give 3-(3,5-dimethyl-4-hydroxybenzoyl)-2-phenylbenzofuran.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03947470 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-692b60dc3866475a8905974a37818000 |
| Source note | uspto-grants-1976_03 |