HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → Diethylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | N-Methylcarbazole | HCID 15142 | — |
| Reactant | 5-Chlorovaleryl chloride | HCID 74089 | — |
| Reactant | 3,6-Bis(4-chlorobutyryl)-N-ethylcarbazole | HCID 12331790 | — |
| Reactant | 3,6-bis(5-chlorovaleryl)-N-methylcarbazole | HCID 21552312 | — |
| Product | Diethylamine | HCID 8021 | — |
| Product | 3,6-bis(5-diethylaminovaleryl)-N-methylcarbazole | HCID 21552359 | — |
Reaction Steps
Following the procedure of Example 32, only substituting respectively for 3,6-bis(4-chlorobutyryl)-N-ethylcarbazole and dimethylamine the appropriate molar equivalent amount of 3,6-bis(5-chlorovaleryl)-N-methylcarbazole, prepared from N-methylcarbazole and 5-chlorovaleryl chloride, and an excess of diethylamine, 3,6-bis(5-diethylaminovaleryl)-N-methylcarbazole is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03947593 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-e563b236db204950bf679886ff1cad90 |
| Source note | uspto-grants-1976_03 |