Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 26891Generated: October 25, 2026

1,3-Propanediamine → HCID 178511125, compound

https://huagongshe.com/reaction/26891

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,3-PropanediamineHCID 428—
ReactantSodium ethoxideHCID 2723922—
ReactantHCID 178478410HCID 178478410—
SolventEthanolHCID 702—
ProductHCID 178511125HCID 178511125—

Reaction Steps

A mixture of 3-chloro-1,2,4-triazole (10.3 g., 0.1 m.) and 1,3-diaminopropane (7.4 g., 0.1 m.) in ethanol containing sodium ethoxide is allowed to stand overnight. The solvent is removed to give 3-(3-aminopropylamino)-1,2,4-triazole. This intermediate is reacted with methyl isothiocyanate to give N-methyl-N'-[3-(3-(1,2,4-triazolyl)amino)propyl]thiourea.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04151288
Source datasetuspto-grants-1979_04
ORD IDord-c7da510a76ce41419b78f6b5d93eb099
Source noteuspto-grants-1979_04