HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanolamine → HCID 43501995, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | 5-Bromo-2-methylbenzene-1-sulfonyl chloride | HCID 4962163 | — |
| Product | HCID 43501995 | HCID 43501995 | 58% |
Reaction Steps
Prepared by general procedure III from 5-Bromo-2-methyl-benzenesulfonyl chloride (1.6 g, 6 mmol, synthesized according to J. Am. Chem. Soc., 1940, 62, 511-514) and ethanolamine (1.0 mL, 17 mmol) to give the title compound (1.02 g, 58%) as a pale-yellow solid. MS (ISP) 294.1[(M+H)+], 296.2[(M+2+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07446113B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-fed2ce371bb1420398239d704e0e7461 |
| Source note | uspto-grants-2008_11 |