HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → 4-Bromo-N,N-dimethylbenzenesulphonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | p-Bromobenzenesulfonyl chloride | HCID 7396 | — |
| Product | 4-Bromo-N,N-dimethylbenzenesulphonamide | HCID 12818 | 77% |
Reaction Steps
Prepared by general procedure III from 4-bromobenzenesulfonyl chloride (9.59 g, 38 mmol) and excess aq. dimethylamine to give the title compound (7.61 g, 77%) as a white crystalline solid. MS (ISP) 266.1[(M+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07446113B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-492a9d2e985445f196e5384122d685f0 |
| Source note | uspto-grants-2008_11 |