N,N-Dimethylethylenediamine → HCID 67000896, compound

HRID 268956Notes

Reaction equation

HRID 268956 reaction equation
[Br:1][C:2]1[C:3]([F:13])=[CH:4][C:5]([F:12])=[C:6]([S:8](Cl)(=[O:10])=[O:9])[CH:7]=1.[CH3:14][N:15]([CH3:19])[CH2:16][CH2:17][NH2:18]>>[Br:1][C:2]1[C:3]([F:13])=[CH:4][C:5]([F:12])=[C:6]([S:8]([NH:18][CH2:17][CH2:16][N:15]([CH3:19])[CH3:14])(=[O:10])=[O:9])[CH:7]=1

Participants

3

Reactant 2

HCID 66053N,N-DimethylethylenediamineHCID 27732965-bromo-2,4-difluorobenzenesulfonyl chloride

Product 1

HCID 67000896HCID 67000896, compoundYield 101.1%

Procedure

Prepared by general procedure III from 5-bromo-2,4-difluorobenzene sulfonyl chloride (1.0 g, 3.4 mmol) and N,N-Dimethylethylenediamine (333 mg, 3.77 mmol) to give the title compound (1.18 g, 100%) as an off-white solid. MS (ISP) 344.9[(M+H)+].

Sources & evidence

ORD record
ord-97a9f28152b34c2982f5e0c3de8f450a
Source dataset
uspto-grants-2008_11
Patent number
US07446113B2

Reaction notes

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