HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodine chloride → 6-(4-Chloro-phenyl)-3-iodo-8-methyl-imidazo[1,2-a]pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodine chloride | HCID 24640 | — |
| Reactant | 6-(4-Chloro-phenyl)-8-methyl-imidazo[1,2-a]pyridine | HCID 67000262 | — |
| Product | 6-(4-Chloro-phenyl)-3-iodo-8-methyl-imidazo[1,2-a]pyridine | HCID 67000648 | 79% |
Reaction Steps
Prepared from 6-(4-chloro-phenyl)-8-methyl-imidazo[1,2-a]pyridine (example C.21 step 1) (6.65 g, 27 mmol) and iodine monochloride as described in example C.20 step 3. Obtained the title compound as an off-white solid (8.0 g, 79%). MS (ISP) 369.0 [(M+H)+], 371 [(M+2+H) +].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07446113B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-3866fd4b37274e4aa4bc6e712a4a6612 |
| Source note | uspto-grants-2008_11 |