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HRID26913

反应详情

EQUATION

反应方程式

HRID 26913 的结构方程式

REACTANTS

反应物

2
结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：CCOC(=O)CC(C)(O)c1ccc(-c2ccc(Br)cc2Br)cc1
HCID53655383

未命名化合物

PRODUCTS

生成物

1
结构：CC(O)(CC(=O)O)c1ccc(-c2ccc(Br)cc2Br)cc1
HCID21322589

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

1 g. of 3-(2',4'-dibromo-4-biphenylyl)-3-hydroxybutyric acid ethyl ester and 0.5 g. of potassium carbonate in 25 ml. of methanol are heated under reflux for one hour and the mixture is worked up to give 3-(2',4'-dibromo-4-biphenylyl)-3-hydroxybutyric acid, m.p. 118°-120°.

WORKUP

后处理

  1. temperatureunder reflux for one hour