HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18936081, compound → HCID 18936072, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18936081 | HCID 18936081 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 18936072 | HCID 18936072 | — |
Reaction Steps
A mixture of 1 g of 1-phosphono-2-(3-pyridinylamino)ethanesulfonic acid and 0.5 g of palladium on charcoal catalyst in 50 ml of distilled water is hydrogenated on a Parr apparatus at 40 PSI for about 2 days. The catalyst is removed by filtration, and the filtrate is concentrated to a few mls. Ethanol is added slowly to precipitate a solid, which is recrystallized from water/ethanol to afford 1-phosphono-2-(3-piperidinylamino)ethanesulfonic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05731299 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-f8cd4bb1e8724101af770fd96846b25d |
| Source note | uspto-grants-1998_03 |