HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-2-thiophenesulfonamide → HCID 67001042, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-2-thiophenesulfonamide | HCID 1241304 | — |
| Reactant | 5-(4-Chloro-phenyl)-3-ethynyl-pyrazolo[1,5-a]pyrimidine | HCID 86608048 | — |
| Product | HCID 67001042 | HCID 67001042 | — |
Reaction Steps
The title compound was prepared from 5-(4-chloro-phenyl)-3-ethynyl-pyrazolo[1,5-a]pyrimidine (example C.6) (37 mg, 0.17 mmol) and 5-bromo-thiophene-2-sulfonamide (35 mg, 0.17 mmol) according to general procedure II. Obtained as a yellow solid (45 mg, 74%). MS (ISP) 415.0 [(M+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07446113B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-4d4fd2c0b0544b02964053a1771299e7 |
| Source note | uspto-grants-2008_11 |