HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → N-[5-methanesulfonyl-4-(4-methanesulfonyl-3-pentafluorosulfanylphenoxy)-2-methylbenzoyl]guanidine, hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 178428844 | HCID 178428844 | — |
| Product | N-[5-methanesulfonyl-4-(4-methanesulfonyl-3-pentafluorosulfanylphenoxy)-2-methylbenzoyl]guanidine, hydrochloride | HCID 178428845 | — |
Reaction Steps
400 mg of N-[5-methanesulfonyl-4-(4-methanesulfonyl-3-pentafluorosulfanylphenoxy)-2-methylbenzoyl]guanidine were dissolved in dilute aqueous HCl solution and then the volatiles were removed in vacuo. The residue was recrystallized from water to result in 200 mg of a pale gray solid, mp 275° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07446225B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-c8b67a8e58ba454eb255bef2afecc3f3 |
| Source note | uspto-grants-2008_11 |