HRID269421

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID313

Hydrochloric Acid

ClH

结构：Cc1cc(Oc2ccc(S(C)(=O)=O)c(S(F)(F)(F)(F)F)c2)c(S(C)(=O)=O)cc1C(=O)NC(=N)N

HCID178428844

未命名化合物

PRODUCTS

生成物

结构：Cc1cc(Oc2ccc(S(C)(=O)=O)c(S(F)(F)(F)(F)F)c2)c(S(C)(=O)=O)cc1C(=O)NC(=N)N.Cl

HCID178428845

未命名化合物

PROCEDURE

实验过程

400 mg of N-[5-methanesulfonyl-4-(4-methanesulfonyl-3-pentafluorosulfanylphenoxy)-2-methylbenzoyl]guanidine were dissolved in dilute aqueous HCl solution and then the volatiles were removed in vacuo. The residue was recrystallized from water to result in 200 mg of a pale gray solid, mp 275° C.

WORKUP

后处理

customthe volatiles were removed in vacuo
customThe residue was recrystallized from water