Lawesson's reagent → HCID 59832201, compound

Participants

Reaction Steps

To a solution of 5-bromo-1H-pyrrolo[2,3-b]pyridine-3-carboxylic acid (2,3-difluoro-phenyl)-amide (300 mg, 0.85 mmol) in toluene (6 mL) was added Lawesson's reagent (210 mg, 0.52 mmol). The suspension was heated under reflux for 14 h. The solvent was removed by evaporation and the residue was dried on the pump for the next reaction. MS (ES+): m/e=368 (M+H); LC: 3.6 min.

Provenance & Evidence