HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 178478222, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Benzyloxy-5-chlorobenzeneboronic acid | HCID 4198740 | — |
| Reactant | Toluene ethanol | HCID 21863594 | — |
| Reactant | HCID 178419370 | HCID 178419370 | — |
| Catalyst | HCID 178418397 | HCID 178418397 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178478222 | HCID 178478222 | — |
Reaction Steps
A mixture of 5-(2′-bromo-biphenyl-3-yl)-1H-tetrazole (163 mg, 0.54 mmol), 2-benzyloxy-5-chlorobenzeneboronic acid (156 mg, 0.59 mmol), potassium carbonate (589 mg, 4.33 mmol), and tetrakis(triphenylphosphine)palladium(0) (63 mg, 0.05 mmol) in 1.1 toluene/ethanol (5 ml) was stirred and heated under nitrogen for 16 hours. After cooling the mixture was diluted with dichloromethane and water. The organic phase was dried and evaporated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07446222B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-e093f7ef662441fb9de78c88b9438a19 |
| Source note | uspto-grants-2008_11 |