Hydrochloric Acid → HCID 86619419, compound

Participants

Reaction Steps

210 mg (0.19 mmol) of the compound from Example 66A are dissolved in 2 ml of THF, and 1 ml each of water and methanol are added. After the addition of 13 mg (0.56 mmol) of lithium hydroxide the mixture is stirred at RT for 12 h. The reaction solution is then diluted with 30 ml of water and adjusted to pH=3 by adding 1N hydrochloric acid. The precipitate is collected by filtration and dried under high vacuum.

Provenance & Evidence