HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Azide → HCID 57440193, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | (2S)-2,4-Bis[(tert-butoxycarbonyl)amino]butyl methanesulphonate | HCID 86601681 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 57440193 | HCID 57440193 | — |
Reaction Steps
Preparation takes place in analogy to Example 85A from 200 mg (0.52 mmol) of (2S)-2,4-bis[(tert-butoxycarbonyl)amino]butyl methanesulfonate (Example 90A) in 15 ml of dimethylformamide with 34 mg (0.52 mmol) of sodium azide. The product is reacted without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07446102B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-ed6e1752664143da84ba51e770eab8e0 |
| Source note | uspto-grants-2008_11 |