HRID269625

反应详情

EQUATION

反应方程式

HRID 269625 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

38 mg (0.12 mmol) of the compound from Example 98A are dissolved in 10 ml of methanol, and 10 mg of palladium on activated carbon (10%) are added. The mixture is hydrogenated under atmospheric pressure for 2 h and filtered through kieselguhr, and the mother liquor is concentrated in vacuo.

WORKUP

后处理

  1. filtrationfiltered through kieselguhr
  2. concentrationthe mother liquor is concentrated in vacuo