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HRID269647

反应详情

EQUATION

反应方程式

HRID 269647 的结构方程式

REACTANTS

反应物

1
结构：CC(C)(C)OC(=O)NCCC[C@@H](CNC(=O)CNC(=O)OCc1ccccc1)NC(=O)OC(C)(C)C
HCID86624495

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)NCCC[C@@H](CNC(=O)CN)NC(=O)OC(C)(C)C
HCID86624496

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Pd]
催化剂HCID23938

Palladium

Pd

结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

Preparation takes place in analogy to Example 81A from 105 mg (0.21 mmol) of benzyl[2-({(2S)-2,5-bis[(tert-butoxycarbonyl)amino]pentyl}amino)-2-oxoethyl]carbamate (Example 125A) in 50 ml of ethanol with the addition of 11 mg of palladium on activated carbon (10%). The product is reacted without further purification.

WORKUP

后处理

  1. customPreparation
  2. customThe product is reacted without further purification