HCID 69219291, compound → HCID 86619438, compound

Participants

Reaction Steps

0.58 g (0.80 mmol) of the compound from Example 228A are dissolved in 27 ml of ethanol, and 0.06 g (0.06 mmol) of Pd/C are added. The mixture is hydrogenated under atmospheric pressure for 12 h and, after filtration through celite, the filtrate is concentrated in vacuo. The solid obtained in this way is reacted further without purification.

Provenance & Evidence