HCID 86619454, compound → HCID 86619453, compound

Participants

Reaction Steps

1030 mg (1.82 mmol) of the compound from Example 263A are dissolved in 60 ml of ethanol, and 100 mg (0.09 mmol) of Pd/C (10%) are added. The mixture is hydrogenated under atmospheric pressure overnight and, after filtration through celite, the filtrate is concentrated in vacuo. The solid obtained in this way is reacted further without purification.

Provenance & Evidence