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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 269692Generated: October 29, 2026

HCID 131727172, compound → HCID 86619455, compound

https://huagongshe.com/reaction/269692

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 131727172HCID 131727172—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 86619455HCID 86619455—

Reaction Steps

355 mg (0.5 mmol) of the compound from Example 267A are dissolved in 17 ml of ethanol, and 36 mg (0.03 mmol) of Pd/C (10%) are added. The mixture is hydrogenated under atmospheric pressure overnight and, after filtration through celite, the filtrate is concentrated in vacuo. The solid obtained in this way is reacted further without purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07446102B2
Source datasetuspto-grants-2008_11
ORD IDord-63615a8a482744e381d8d89b9825702b
Source noteuspto-grants-2008_11