HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131727172, compound → HCID 86619455, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131727172 | HCID 131727172 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86619455 | HCID 86619455 | — |
Reaction Steps
355 mg (0.5 mmol) of the compound from Example 267A are dissolved in 17 ml of ethanol, and 36 mg (0.03 mmol) of Pd/C (10%) are added. The mixture is hydrogenated under atmospheric pressure overnight and, after filtration through celite, the filtrate is concentrated in vacuo. The solid obtained in this way is reacted further without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07446102B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-63615a8a482744e381d8d89b9825702b |
| Source note | uspto-grants-2008_11 |