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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 269705Generated: October 28, 2026

Hydrochloric Acid → HCID 66879422, compound

https://huagongshe.com/reaction/269705

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 89225972HCID 89225972—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 66879422HCID 66879422—

Reaction Steps

0.32 ml of a 4N solution of hydrogen chloride in dioxane are added to a solution of 25 mg (0.021 mmol) of the compound from Example 262A in 1 ml of dioxane at 0° C. After 2 h at RT, the reaction solution is concentrated in vacuo and coevaporated with dichloromethane several times. The remaining solid is dried to constant weight under high vacuum.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07446102B2
Source datasetuspto-grants-2008_11
ORD IDord-06c1eb68942a4e15830b7e66d07ba556
Source noteuspto-grants-2008_11