HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 66879422, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 89225972 | HCID 89225972 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 66879422 | HCID 66879422 | — |
Reaction Steps
0.32 ml of a 4N solution of hydrogen chloride in dioxane are added to a solution of 25 mg (0.021 mmol) of the compound from Example 262A in 1 ml of dioxane at 0° C. After 2 h at RT, the reaction solution is concentrated in vacuo and coevaporated with dichloromethane several times. The remaining solid is dried to constant weight under high vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07446102B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-06c1eb68942a4e15830b7e66d07ba556 |
| Source note | uspto-grants-2008_11 |