4-Hydroxybiphenyl → HCID 178460475, compound

HRID 269710Notes

Reaction equation

HRID 269710 reaction equation
C1([C:7]2[CH:12]=[CH:11][C:10]([OH:13])=[CH:9][CH:8]=2)C=CC=CC=1.[CH2:14]([CH:19]1[CH2:24][CH2:23][CH:22]([C:25]2[CH:30]=[CH:29][C:28]([OH:31])=[CH:27][CH:26]=2)[CH2:21][CH2:20]1)[CH2:15][CH2:16][CH2:17][CH3:18]>>[CH2:14]([C@H:19]1[CH2:20][CH2:21][C@H:22]([C:25]2[CH:26]=[CH:27][C:28]([O:31][CH2:11][CH2:12][CH2:7][CH2:8][CH2:9][CH2:10][O:13][C:10](=[O:13])[CH:9]=[CH2:8])=[CH:29][CH:30]=2)[CH2:23][CH2:24]1)[CH2:15][CH2:16][CH2:17][CH3:18]

Participants

3

Reactant 2

HCID 71034-HydroxybiphenylHCID 45937654-(4-Pentylcyclohexyl)phenol

Product 1

HCID 178460475HCID 178460475, compound

Procedure

With the exception of replacing the 4-phenylphenol from the synthesis example 1 with 4-(4-pentylcyclohexyl)phenol, 19.4 g of a monoacrylate containing a group (h): 1-pentyl-4-(4-(6-acryloyloxyhexyloxy)phenyl)trans-cyclohexane was obtained in the same manner as the synthesis example 1. Hereafter this monoacrylate is abbreviated as (A-3).

Sources & evidence

ORD record
ord-67365448f44a481191f156b37fbbfada
Source dataset
uspto-grants-2008_11
Patent number
US07449223B2

Reaction notes

Loading…