HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(4-Methoxy-2-methylphenyl)-4-phenethylpiperazine → HCID 23111433, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(4-Methoxy-2-methylphenyl)-4-phenethylpiperazine | HCID 23111468 | — |
| Reactant | 1-(4-Methoxy-3-methylphenyl)-4-phenethylpiperazine | HCID 23111510 | — |
| Product | HCID 23111433 | HCID 23111433 | 85.3% |
Reaction Steps
Production Example 10 was repeated except that 1-(4-methoxy-3-methylphenyl)-4-phenethylpiperazine was replaced with 1-(4-methoxy-2-methylphenyl)-4-phenethylpiperazine (512 mg), and the resulting crude product was purified on TLC (developer, chloroform: methanol=15:1) to provide 3-methyl-4-(4-phenethyl-piperazin-1-yl)phenol (417 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07449466B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-dd4ec3476b8746cfaacddae4450b0b2f |
| Source note | uspto-grants-2008_11 |