HRID269873

反应详情

EQUATION

反应方程式

HRID 269873 的结构方程式

PROCEDURE

实验过程

Production Example 10 was repeated except that 1-(4-methoxy-3-methylphenyl)-4-phenethylpiperazine was replaced with 5-methoxy-2-(4-phenylpiperidino)benzonitrile (99 mg), and the resulting crude product was purified on TLC (developer, hexane: ethyl acetate=2:1) to provide 5-hydroxy-2-(4-phenylpiperidino)benzonitrile (42 mg).

WORKUP

后处理

  1. customthe resulting crude product was purified on TLC (developer, hexane: ethyl acetate=2:1)