HRID269878

反应详情

EQUATION

反应方程式

HRID 269878 的结构方程式

PROCEDURE

实验过程

Production Example 10 was repeated except that 1-(4-methoxy-3-methylphenyl)-4-phenethylpiperazine was replaced with 2-[4-(3-cyclohexylpropyl)piperazin-1-yl]-5-methoxybenzonitrile (430 mg), and the resulting crude product was purified on TLC (developer, chloroform: methanol=10:1) to provide 2-[4-(3-cyclohexylpropyl)piperazin-1-yl]-5-hydroxybenzonitrile (256 mg).

WORKUP

后处理

  1. customthe resulting crude product was purified on TLC (developer, chloroform: methanol=10:1)