HRID269884

反应详情

EQUATION

反应方程式

HRID 269884 的结构方程式

PROCEDURE

实验过程

Production Example 28 was repeated except that 1-(3-chloro-4-methoxymethoxyphenyl)-4-phenethylpiperazine was replaced with 2-[4-(3-chloro-4-methoxymethoxyphenyl)piperazin-1-yl]-1-phenylethan-1-one (221 mg). Thus obtained crude product was purified on TLC (developer, chloroform: acetone=6:1) to provide 2-[4-(3-chloro-4-hydroxyphenyl)piperazin-1-yl]-1-phenylethan-1-one (26 mg).

WORKUP

后处理

  1. customThus obtained crude product
  2. customwas purified on TLC (developer, chloroform: acetone=6:1)