HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3-Chloro-4-methoxymethoxyphenyl)-4-phenethylpiperazine → HCID 23111407, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3-Chloro-4-methoxymethoxyphenyl)-4-phenethylpiperazine | HCID 23111442 | — |
| Reactant | 2-[4-(3-Chloro-4-methoxymethoxyphenyl)piperazin-1-yl]-1-phenylethan-1-one | HCID 23111474 | — |
| Product | HCID 23111407 | HCID 23111407 | 13.3% |
Reaction Steps
Production Example 28 was repeated except that 1-(3-chloro-4-methoxymethoxyphenyl)-4-phenethylpiperazine was replaced with 2-[4-(3-chloro-4-methoxymethoxyphenyl)piperazin-1-yl]-1-phenylethan-1-one (221 mg). Thus obtained crude product was purified on TLC (developer, chloroform: acetone=6:1) to provide 2-[4-(3-chloro-4-hydroxyphenyl)piperazin-1-yl]-1-phenylethan-1-one (26 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07449466B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-0a72113bee674439ab4fb80d70472753 |
| Source note | uspto-grants-2008_11 |