HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylcarbamoyl chloride → HCID 23111441, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylcarbamoyl chloride | HCID 6916 | — |
| Reactant | Isovaleryl chloride | HCID 66054 | — |
| Reactant | 1-(4-Methoxyphenyl)-piperazine, dihydrochloride | HCID 2723700 | — |
| Reactant | 1-(4-Benzyloxy-3-fluorophenyl)piperazine | HCID 23111483 | — |
| Product | HCID 23111441 | HCID 23111441 | — |
Reaction Steps
Production Example 3 was repeated except that 1-(4-methoxyphenyl)-piperazine dihydrochloride and isovaleryl chloride were replaced with 1-(4-benzyloxy-3-fluorophenyl)piperazine (286 mg) and diethylcarbamoyl chloride (139 μL), respectively, to provide crude N,N-diethyl-4-(4-benzyloxy-3-fluorophenyl)-1-piperazinecarboxamide (370 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07449466B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-01b03a2f77a643f98084a469ef708001 |
| Source note | uspto-grants-2008_11 |