HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23111498, compound → HCID 23111472, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23111498 | HCID 23111498 | — |
| Reactant | 1-(4-Methoxy-3-methylphenyl)-4-phenethylpiperazine | HCID 23111510 | — |
| Product | HCID 23111472 | HCID 23111472 | 39.6% |
Reaction Steps
Production Example 10 was repeated except that 1-(4-methoxy-3-methylphenyl)-4-phenethylpiperazine was replaced with 1-decyl-4-(2,5-difluoro-4-methoxyphenyl)piperazine (176 mg). The resulting crude product was purified on TLC (developer, chloroform: methanol=19:1) to provide 4-(4-decylpiperazin-1-yl)-2,5-difluorophenol (67 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07449466B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-c09401c6674e49d9bdbb3ac59c838c94 |
| Source note | uspto-grants-2008_11 |