HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 11387449, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 58812046 | HCID 58812046 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 11387449 | HCID 11387449 | — |
Reaction Steps
Bubble gaseous HCl through a solution of [3-(4-Nitro-phenyl)-propyl]-[2-(7-phenyl-isoquinoline-5-sulfonylamino)-ethyl]-carbamic acid tert-butyl ester (1.9 g, 2.9 mmol) in methanol/dichloromethane (1:1) with cooling for 15 minutes. Remove the solvent under reduced pressure to afford the title compound as a foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07449477B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-0a8f02ce0f764b849be622bf1c3420ca |
| Source note | uspto-grants-2008_11 |