HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopropylamine → HCID 28390698, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopropylamine | HCID 69828 | — |
| Reactant | Methyl 4-methoxysalicylate | HCID 79523 | — |
| Product | HCID 28390698 | HCID 28390698 | — |
Reaction Steps
A suspension of methyl 2-hydroxy-4-methoxybenzoate (5.1 g, 28.0 mmol) in cyclopropyl amine 24 mL) was stirred at room temperature for 5 days. The volatiles were removed in vacuo and the residue was purified by silica gel flash chromatography (0-60% ethyl acetate in petroleum ether) to give the subtitled compound (1.8 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07449475B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-28b3b4d48a0f4850b7c740c5ce9c9a29 |
| Source note | uspto-grants-2008_11 |