HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopropylamine → HCID 68960505, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopropylamine | HCID 69828 | — |
| Reactant | HCID 14999687 | HCID 14999687 | — |
| Product | HCID 68960505 | HCID 68960505 | — |
Reaction Steps
Methyl 2-hydroxy-4-(trityloxy)benzoate (340 mg, 0.83 mmol) was dissolved in cyclopropylamine (3 mL) and left at room temperature for a week. The volatiles were removed in vacuo and the residue was purified by silica gel flash chromatography (0-20% ethyl acetate in petroleum ether) to give the subtitled compound (210 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07449475B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-a0946a8150fa4d058ac1b164d173ed30 |
| Source note | uspto-grants-2008_11 |