HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 68959972, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | Benzoic acid, 2-hydroxy-4-[(4-methoxyphenyl)methoxy]-, methyl ester | HCID 10541338 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 68959972 | HCID 68959972 | — |
Reaction Steps
To a suspension of methyl 2-hydroxy-4-[(4-methoxybenzyl)oxy]benzoate (500 mg, 1.73 mmol) in methanol (15 mL) was slowly added aqueous 40% methylamine (3 mL) at 0° C. After addition was complete the reaction mixture was kept on stirring at room temperature for 2 days. The volatiles were removed in vacuo to give the subtitled compound (500 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07449475B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-d2ac80437a044b00b4b6549ecd25c007 |
| Source note | uspto-grants-2008_11 |