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HRID270104

反应详情

EQUATION

反应方程式

HRID 270104 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)C(F)(F)F
HCID6422

未命名化合物

结构：CC(C)(C)OC(=O)N1CC[C@H](OC(=O)c2ccccc2)C1
HCID15117240

未命名化合物

PRODUCTS

生成物

1
结构：O=C(O[C@H]1CCNC1)c1ccccc1
HCID11160511

未命名化合物

收率 191.9%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

tert-Butyl(3S)-3-(benzoyloxy)pyrrolidine-1-carboxylate (635 mg, 2.18 mmol) was treated with 20% CF3CO2H in CH2Cl2 (20 mL) overnight at room temperature. The volatiles were removed in vacuo to give the subtitled compound (800 mg).

WORKUP

后处理

  1. customThe volatiles were removed in vacuo