HCID 59833546, compound → HCID 59833561, compound

Participants

Reaction Steps

tert-Butyl 5-(trifluoromethyl)-3′,6′-dihydro-3,4′-bipyridine-1′(2′H)-carboxylate (50.0 mg, 0.152 mmol) was dissolved in a 4 M solution of HCl in 1,4-dioxane (2 mL) to form a light yellow clear (then cloudy) solution. After being stirred at room temperature for 1 h, the reaction mixture was concentrated in vacuo to afford 40.0 mg (87%) of product as a yellow gum. LC-MS calculated for C11H11F3N2: (M+H) 229; found 229.0.

Provenance & Evidence