HRID270780

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID8000

Ethane, 1,1'-oxybis-, compd. with trifluoroborane (1:1)

C4H10BF3O

HCID9321

Hydrazine

H4N2

HCID9794

Ethyl trifluoroacetate

C4H5F3O2

HCID69019

3-Methylbut-1-yne

C5H8

HCID178418339

Butyllithium

C4H9Li

PRODUCTS

生成物

HCID23006214

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID241

Benzene

C6H6

溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

Following protocol H, 3-methylbutyne was treated with n-BuLi, CF3CO2Et and BF3—OEt2 in THF. Reaction with hydrazine in benzene under similar reaction conditions yielded title compound.

WORKUP

后处理

customunder similar reaction conditions