HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 21071039, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-(Chloroacetyl)-4-(4-fluorophenyl)piperazine | HCID 1848511 | — |
| Reactant | HCID 21071132 | HCID 21071132 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 21071039 | HCID 21071039 | — |
Reaction Steps
Protocol T was followed using 3,5-Diisopropyl-4-chloro-1H-pyrazole, K2CO3, 2-Chloro-1-[4-(4-fluoro-phenyl)-piperazin-1-yl]-ethanone and DMF. Column chromatography using a solvent mixture (hexane/ethyl acetate=1/1, Rf=0.76) afforded the title compound as white solid. MS (ES) M+H) expected=406.9, found 407.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07449576B1 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-a8528cc28cc94323ab3c1506d36fd338 |
| Source note | uspto-grants-2008_11 |