HRID271032

反应详情

EQUATION

反应方程式

HRID 271032 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

In another preparation, a 5.00 g sample of fluoxetine HCl and 1.76 g of benzoic acid were dissolved in 50 mL of acetonitrile with heating. The solution was allowed to crystallize in a large evaporating dish. The resulting solid was isolated on filter paper and dried in the air to yield 5.40 g (92%) of fluoxetine HCl:benzoic acid (1:1) cocrystal.

WORKUP

后处理

  1. customIn another preparation
  2. temperaturewith heating
  3. customto crystallize in a large evaporating dish
  4. customThe resulting solid was isolated
  5. filtrationon filter paper
  6. customdried in the air