HuagongsheHuagongshe Chemistry Print Report · For research reference only
Succinic Acid → HCID 131727182, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Succinic Acid | HCID 1110 | — |
| Reactant | Reconcile | HCID 62857 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 131727182 | HCID 131727182 | 92% |
Reaction Steps
In another preparation, a 5.00 g sample of fluoxetine HCl and 0.85 g of succinic acid were dissolved in acetonitrile with heating. The solution was allowed to crystallize in an open evaporating dish over a 15 minute period. The solid material was isolated on filter paper and dried to yield 5.40 g (92% yield) of fluoxetine HCl:succinic acid (2:1) cocrystal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07452555B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-b66b8e232b4f4b0c81684e840b6dbdbe |
| Source note | uspto-grants-2008_11 |