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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 27123Generated: October 30, 2026

1,1-Bis(methylthio)-2-nitroethylene → 1-Nitro-2-methylthio-2-[4-(4-imidazolyl)butylamino]ethylene

https://huagongshe.com/reaction/27123

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,1-Bis(methylthio)-2-nitroethyleneHCID 83623—
ReactantHCID 178510963HCID 178510963—
SolventIsopropanolHCID 3776—
Product1-Nitro-2-methylthio-2-[4-(4-imidazolyl)butylamino]ethyleneHCID 178503821—

Reaction Steps

Reaction of 5-bromo-4(4-aminobutyl)imidazole with 1-nitro-2,2-bis-methylthioethylene in the procedure of Example 8(i) yields 1-nitro-2-methylthio-2-[4-(4-imidazolyl)butylamino]ethylene, m.p. 157°-158°, (from isopropanol).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04220652
Source datasetuspto-grants-1980_09
ORD IDord-dc51b310f2da43c4a27864ec87cff893
Source noteuspto-grants-1980_09