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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 271265Generated: October 31, 2026

Benzylamine → HCID 58758771, compound

https://huagongshe.com/reaction/271265

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzylamineHCID 7504—
ReactantBis-(1H-imidazol-2-YL)-methanoneHCID 5250894—
ReactantHCID 59834998HCID 59834998—
SolventWaterHCID 962—
SolventDimethylformamideHCID 6228—
ProductHCID 58758771HCID 5875877166%

Reaction Steps

A suspension of 2-amino-6-(2-furyl)-9H-purine-9-acetic acid (129 mg, 0.5 mmol) in DMF (2 mL) was treated with carbonyl diimidazole (81 mg, 0.5 mmol), stirred at room temperature for 1 h, treated with benzylamine (55 μL, 0.5 mmol), stirred at room temperature for 2 h, diluted with water, filtered and dried to give the title compound (115 mg, 66%) as a white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07452894B2
Source datasetuspto-grants-2008_11
ORD IDord-b6a7f8434d204cc7b5fb1e584bed9c16
Source noteuspto-grants-2008_11