Dabco → HCID 58758763, compound

Participants

Reaction Steps

A solution of 2-chloro-6-(2-furyl)-9-(4-methylbenzyl)-9H-purine (0.10 g, 0.31 mmol) and Et4NCN (0.10 g, 0.62 mmol) in acetonitrile (10 mL) was treated with DABCO (0.07 g, 0.62 mmol), stirred for 48 h, concentrated in vacuo, dissolved in chloroform (50 mL), washed with water (2×30 mL), dried (MgSO4) and concentrated in vacuo to give the title compound (56 mg, 57%) as a pale green solid.

Provenance & Evidence