HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropylamine → HCID 58772830, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropylamine | HCID 6363 | — |
| Reactant | 5-chloro-7,8-bis(4-chlorophenyl)-[1,2,4]triazolo[4,3-c]pyrimidin-3(2H)-one | HCID 58772840 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 58772830 | HCID 58772830 | — |
Reaction Steps
To a stirring solution of 5-chloro-7,8-bis(4-chlorophenyl)-[1,2,4]triazolo[4,3-c]pyrimidin-3(2H)-one (39 mg, 0.10 mmol) in 1 mL THF, was added isopropylamine (18 mg, 0.30 mmol). The reaction mixture was stirred at room temperature for 1 h and then concentrated under reduced pressure. The resulting crude title compound was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07452892B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-fe6ed3745cb84b19b8d45685c6afdf0d |
| Source note | uspto-grants-2008_11 |