HuagongsheHuagongshe Chemistry Print Report · For research reference only
Anthranilamide → HCID 819654, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Anthranilamide | HCID 6942 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Cyclohexanecarbonyl chloride | HCID 75938 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 819654 | HCID 819654 | — |
Reaction Steps
Anthranilamide was treated with cyclohexanecarbonyl chloride and triethylamine in dichloromethane, followed by washing (10% citric acid; water; sat. sodium bicarbonate; and sat. sodium chloride) and evaporated to give a nearly quantitative yield of 2-(cyclohexylcarbonylamino)benzamide as a white solid, which was used immediately in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07452912B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-8948d6da0dd74c0b868e830c3dee5af4 |
| Source note | uspto-grants-2008_11 |