Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 271668Generated: October 31, 2026

HCID 60659962, compound → HCID 62642302, compound

https://huagongshe.com/reaction/271668

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 60659962HCID 60659962—
CatalystNickelHCID 935—
SolventMethanolHCID 887—
ProductHCID 62642302HCID 62642302—

Reaction Steps

100 mg Raney Nickel are added to a solution of 1.00 g (3.18 mmol) (4-bromo-2-nitro-phenyl)-(2-pyrrolidin-1-yl-ethyl)-amine in 100 mL MeOH. The reaction solution is stirred for 15 min at 3 bar H2 and RT. After filtration the solvent is eliminated i.vac. and the product is further reacted without purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07452911B2
Source datasetuspto-grants-2008_11
ORD IDord-3bdfaf628255417c889c3dabee2aa532
Source noteuspto-grants-2008_11