化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → Hydrochloric Acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | N-(3-Azido-5-fluoropyridin-2-yl)-2,2-dimethylpropanamide | HCID 22293288 | — |
| 生成物 | Hydrochloric Acid | HCID 313 | — |
| 生成物 | 3-Azido-5-fluoropyridin-2-amine | HCID 22293242 | — |
反応手順
N-(3-Azido-5-fluoropyridin-2-yl)-2,2-dimethylpropanamide (275 mg, 1.16 mmol) in 3 N HCl (5 mL) was heated to 100° C. After 2 h, the volatiles were removed in vacuo, to give the title compound as its HCl salt (180 mg). MS 154.2 (M+1).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07452903B2 |
| 出典データセット | uspto-grants-2008_11 |
| ORD ID | ord-321efd9e941f4a5a9155c968db9dec32 |
| 出典メモ | uspto-grants-2008_11 |