HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 1-(2,6-Dichlorophenyl)-3-carbamyl-3-methylthiouronium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 1-(2,6-Dichlorophenyl)-3-carbamylthiourea | HCID 20434424 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 1-(2,6-Dichlorophenyl)-3-carbamyl-3-methylthiouronium iodide | HCID 178485195 | — |
Reaction Steps
26.4 g (0.1 mole) of 1-(2,6-dichlorophenyl)-3-carbamylthiourea is combined with 200 ml of methanol and 14.1 g (0.1 mole) of iodomethane and refluxed for 4 hours. This is then evaporated to dryness and 100 ml of hexane is added. The mixture is filtered to obtain 1-(2,6-dichlorophenyl)-3-carbamyl-3-methylthiouronium iodide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04220658 |
| Source dataset | uspto-grants-1980_09 |
| ORD ID | ord-5dd0d1be2a4841c485ed4cea453620ba |
| Source note | uspto-grants-1980_09 |