HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloride methanol → Ethyl 3-{(2-aminoacetyl)amino}propionate monohydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloride methanol | HCID 21893726 | — |
| Reactant | Ethyl 3-(2-{(tert-butoxycarbonyl)amino}acetylamino)propionate | HCID 21893946 | — |
| Product | Ethyl 3-{(2-aminoacetyl)amino}propionate monohydrochloride | HCID 22647362 | — |
Reaction Steps
2.0 Grams of ethyl 3-(2-{(tert-butoxycarbonyl)amino}-acetylamino)propionate were dissolved in 30 ml of 10% hydrochloric acid-methanol and stirred for 15 hours at room temperature. Upon distilling the reaction liquid off under reduced pressure, 1.52 g of the title compound was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07452908B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-2307c7390744429b96f5f0e1f5769833 |
| Source note | uspto-grants-2008_11 |