HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 131727194, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 74016630 | HCID 74016630 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 131727194 | HCID 131727194 | 184.5% |
Reaction Steps
The compound of Example 232 (300 mg) was dissolved in methanol (10 mL) containing 10% hydrochloric acid in an ice bath. The mixture was stirred for 6 hours until room temperature and the solvent was concentrated. This gave the desired product as a colorless oil (250 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07456157B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-a571060c2e3647e08da566c4eecbd8ef |
| Source note | uspto-grants-2008_11 |